Analytical Method Validation Review Checklist [FREE PDF]

This analytical method validation review checklist ensures compliance with ICH Q2(R1) Validation of Analytical Procedures requirements. Analytical Development Scientists use this checklist to verify regulatory compliance, document findings, and maintain safety and quality standards.

  • Industry: Pharmaceutical / Life Sciences
  • Frequency: Per Method
  • Estimated Time: 4-8 hours
  • Role: Analytical Development Scientist
  • Total Items: 21
  • Compliance: ICH Q2(R1) Validation of Analytical Procedures, FDA Guidance for Industry Analytical Methods, USP <1225> Validation of Compendial Methods, ISO/IEC 17025 Laboratory Validation

Documentation and Regulatory Review

Verify required documentation is current and complete.

  • Standard Operating Procedures (SOPs) current and accessible?
  • All personnel training records current for this activity?
  • Required permits, licenses, and registrations current?
  • Previous inspection findings reviewed and corrective actions verified?

Safety and Equipment Requirements

Verify safety equipment, PPE, and emergency preparations.

  • Required PPE available, clean, and in good condition?
  • Emergency equipment (eyewash, shower, extinguisher) accessible?
  • Safety Data Sheets (SDS) available for all hazardous materials?
  • Emergency contact and response procedures posted?

Operational Compliance Checks

Verify operations comply with regulatory requirements.

  • Approved procedures being followed without deviation?
  • Equipment qualified/calibrated and within calibration period?
  • Environmental monitoring (temp, humidity, pressure) within spec?
  • All materials, products, and containers properly labeled?
  • Data recorded contemporaneously with no unexplained alterations?

Waste Disposal and Environmental Compliance

Verify proper waste handling and disposal.

  • All waste properly labeled with contents and hazard class?
  • Waste containers appropriate for waste type and in good condition?
  • Waste streams segregated per regulatory requirements?
  • Waste disposal records maintained?

Findings and CAPA

Document findings and corrective/preventive actions.

  • Any deviations or non-conformances identified?
  • CAPA initiated for any findings?
  • Photo documentation of findings?
  • Inspection findings and recommendations

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Why Use This Analytical Method Validation Review Checklist [FREE PDF]?

This analytical method validation review checklist [free pdf] helps pharmaceutical / life sciences teams maintain compliance and operational excellence. Designed for analytical development scientist professionals, this checklist covers 21 critical inspection points across 5 sections. Recommended frequency: per method.

Ensures compliance with ICH Q2(R1) Validation of Analytical Procedures, FDA Guidance for Industry Analytical Methods, USP <1225> Validation of Compendial Methods, ISO/IEC 17025 Laboratory Validation. Regulatory-aligned for audit readiness and inspection documentation.

Frequently Asked Questions

What does the Analytical Method Validation Review Checklist [FREE PDF] cover?

This checklist covers 21 inspection items across 5 sections: Documentation and Regulatory Review, Safety and Equipment Requirements, Operational Compliance Checks, Waste Disposal and Environmental Compliance, Findings and CAPA. It is designed for pharmaceutical / life sciences operations and compliance.

How often should this checklist be completed?

This checklist should be completed per method. Each completion takes approximately 4-8 hours.

Who should use this Analytical Method Validation Review Checklist [FREE PDF]?

This checklist is designed for Analytical Development Scientist professionals in the pharmaceutical / life sciences industry. It can be used for self-assessments, team audits, and regulatory compliance documentation.

Can I download this checklist as a PDF?

Yes, this checklist is available as a free PDF download. You can also use it digitally in the POPProbe mobile app for real-time data capture, photo documentation, and automatic reporting.

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